TERT-BUTYL P-(BROMOMETHYL) BENZOATE
4-Bromomethyl-benzoic acid tert-butyl ester
CAS: 108052-76-2
Molecular Formula: C12H15BrO2
TERT-BUTYL P-(BROMOMETHYL) BENZOATE - Names and Identifiers
TERT-BUTYL P-(BROMOMETHYL) BENZOATE - Physico-chemical Properties
| Molecular Formula | C12H15BrO2 |
| Molar Mass | 271.15 |
| Density | 1.313±0.06 g/cm3(Predicted) |
| Melting Point | 53-55 °C |
| Boling Point | 320.9±25.0 °C(Predicted) |
| Flash Point | 147.9°C |
| Vapor Presure | 0.000308mmHg at 25°C |
| Appearance | White solid |
| Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
| Refractive Index | 1.537 |
| MDL | MFCD04973450 |
TERT-BUTYL P-(BROMOMETHYL) BENZOATE - Reference Information
| use | tert-butyl 4-bromomethyl benzoate is an intermediate for the synthesis of acaricide acaricide acardol. |
| production method | the preparation method is to add 0.56g tert-butanol, 0.395g pyridine and 1.75g 4-bromomethylbenzoyl chloride to a three-mouth bottle equipped with a stirrer and thermometer, and react at 10~30 ℃ for 5h. After the reaction, add 10mL of water to the reaction bottle, move to the separatory funnel, and extract with ethyl acetate. The extracts were combined, washed with dilute acid, separated into acid water layer and then desoluted under reduced pressure to obtain 0.98g of tert-butyl 4-bromomethylbenzoic acid with 72.0% yield. |
Last Update：2024-04-09 20:52:54
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View History
TERT-BUTYL P-(BROMOMETHYL) BENZOATE
哒嗪-4,5-二醇
2-(Butoxymethyl)furan
(2E)-2-十三碳烯醛
磷酸烯醇丙酮酸单环己铵盐
2-氨基-4-硝基苯甲醚
AURORA KA-2521
莫诺莱特坚牢蓝2RVSA
Kaliumtetrahydridoborat
D-二苯甲酰基酒石酸
哒嗪-4,5-二醇
2-(Butoxymethyl)furan
(2E)-2-十三碳烯醛
磷酸烯醇丙酮酸单环己铵盐
2-氨基-4-硝基苯甲醚
AURORA KA-2521
莫诺莱特坚牢蓝2RVSA
Kaliumtetrahydridoborat
D-二苯甲酰基酒石酸